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In this paper, a systematic investigation into the structureproperty relationship of long-chain N-alkyl amide 1, O-alkyl ester arginine 2, and N-acyl arginine methyl ester analogues 3 is reported. The surface properties were studied by adsorption isotherm curves. Biological properties such as antimicrobial activity, hemolysis, ocular irritation, aquatic toxicity, and biodegradability are